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Autosampler - Model
AS-1555/1555-10
The Model AS-1555 and AS-1555-10 are fully automatic sample
injection systems enabling greater productivity and the highest possible
level of precision. Sampling flexibility is unparalleled with up to 96
well positions (microplate) for laboratory automation and combinatorial
chemistry. Also available is a rack for 84 micro-vials or the standard
rack for 50 2 ml vials. The AS-1555/1555-10 offer 5 operating modes;
normal, two methods of pre-column derivatization, dilution, and
zero-sample loss injection in stand-alone mode. In the zero-sample loss
mode, the sample is sandwiched between two zones of mobile phase solvent,
and the entire sample volume is drawn into the loop and injected without
loss.
The AS-1555 and AS-1555-10 can be easily combined with the HPLC system
and the HSS-1500 software for Windows NT®. The HSS-1500 program
offers full automation of your HPLC system including the autosampler,
along with an audit trail and enhanced GLP compliance. The software also
allows display and document maintenance information of the detector,
analysis log, SOP and results of instrument validation for laboratories in
regulated industries.
Features
Excellent injection reproducibility The AS-1555/1555-10 offer
operation in both fixed loop or variable volume injection modes. The
reproducibility achieved in fixed loop 20 Fl
injection is less than 0.2% SD with less than 0.01% sample contamination.
In variable 10 Fl injections SD was less than
0.3%.
Complete flexibility Random sample access is provided as well as
random number of injections and random injection volume for each vial.
Urgent samples can be given priority.
Temperature control (AS-1555-10 only) The AS-1555-10 offers a
built-in Peltier cooling and heating unit to expand the versatility of the
instrument and maintain the integrity of all samples.
Non-adsorbent tubing The AS-1555/1555-10 both use an innovative
stainless steel tubing, eliminating the adsorption problem than occurs
when analyzing natural samples using Teflon tubing.
Sample pretreatment capability Air segmented sampling enables
the AS-1555 and AS-1555-10 to automatically mix up to two different
solvents or derivatizing reagents with the sample in a stand-alone mode.
By automating the processes of derivatizations, the sample pretreatment
capability saves time and improves the precision of complex
chromatographic analyses.
Interfacing with the HPLC system The AS-1555/1555-10 can be used
as stand-alone module through the built-in keypad and LCD display, or
integrated into a complete HPLC system with computer control. In
stand-alone mode, the advanced microprocessor of the AS-1555/1555-10 offer
10 user friendly programs with 64 steps per program. The AS-1555/1555-10
can freely interact with other HPLC modules via the built-in LC-Net
interface and can also easily be triggered from an external event
generated by a computer or other LC modules. Full PC control is also
provided when incorporated in a HPLC system with our new 3 bit HSS-1500
HPLC System control software for Windows NT®.
GLP/GMP compliance The AS-1555/1555-10 were designed keeping
GLP/GMP compliance in mind. Various GLP/GMP parameters including serial
number, number of injections and number of suctions, are displayed in the
LCD display. Utilizing the 32 bit HSS-1500 HPLC System control software,
this GLP/GMP information is stored in a database along with an analysis
log. Instrument validation can also be easily performed according to an
electronic Standard Operation Procedure (SOP) provided with the HSS-1500
program. Test results of validation are recorded manually, and the results
obtained are automatically compared with acceptable criteria set by user.
The results can be printed for hard copy documentation along with the SOP.
These various functions allow users to fully comply with GLP/GMP
requirements.
Specifications |
Sampling
mode |
Partial (variable
volume) or full (fixed) loop loading selectable |
Number of
sample |
50 for standard 2
ml vials 84 for 0.6 and 0.3 ml vials 96 for
microplate |
Sample
loop |
100 Fl standard |
Injection
volume Variable mode |
0.1 -200 Fl (standard), 1 - 2000 Fl (optional) |
Fixed
mode |
100 Fl (standard) |
Others
loops |
5, 10, 20, 50,
200, 500, 1000, 2000 and 5000 Fl are
available as optional accessory. |
Reproducibility |
0.3% c.v.
(Variable injection of 10 Fl) 0.2% c.v. (Fixed
injection of 20 Fl) |
Cross
contamination |
0.01% (20 Fl injection) |
Sample
loss |
10 Fl (5 ~ 100 Fl) |
Sample
rack |
50 sample position
(Chromacol SV-2 vial) 84 sample position
(Chromacol 0.3-CVG, 0.2-CTV as option 96 position
microplate as option |
Temperature control |
+ 4 EC and + 37 EC
by Peltier cooling unit built-in (AS-1555-10 only) |
Maximum
operating pressure |
35
MPa |
Liquid
wetted materials |
SUS-316,
fluoropolymer and glass |
Operation |
Through
interactive key operation with keypad |
Operating
mode |
Normal
mode Pre-column derivatization mode
1 Pre-column derivatization mode
2 Dilution mode Zero-sample loss
injection mode |
Program
function |
Sample nos.,
range, injection volume, No. of infections can be programmed in max.
64 steps. 10 such program files are avalaible and
stored. |
Self-diagnostics |
Memory (ROM,RAM),
DC power supply and mechanical parts Inputs and
outputs |
Infection
markers |
3 contact closures
signals |
STOP
OUT |
1 |
STOP
IN |
1 |
REMOTE
INJ. |
1 |
Dimensions |
AS-1555 |
150 (W) x 470 (D)
x 307 (H) mm, approx. 12 kg |
AS-1555-10 |
150 (W) x 470 (D)
x 387 (H) mm, approx. 16 kg |
Power
requirements |
AS-1555 |
150
VA |
AS-1555-10 |
250
VA |
|
|
CAT.
NO. |
DESCRIPTION |
6777-J005A |
Model AS-1555
Autosampler |
6777-J006A |
Model AS-1555-10
Autosampler |
6777-J004A |
Model AS-1550
Autosampler |
6778-J002A |
Model PU-1580 HPLC
Pump |
6778-J004A |
Model PU-986
Semipreparative HPLC Pump |
6778-J006A |
Model PU-987 Preparative
HPLC Pump |
6779-J004A |
Model UV-1575 UV/VIS
Detector |
6779-J002A |
Model UV-1570 UV/VIS
Detector |
6781-J002A |
Model MD-1510
Multiwavelenght UV/VIS Detector (~ 650 nm) |
6781-J002A |
Model MD-1515
Multiwavelenght UV/VIS Detector (~ 900 nm) |
6780-J002A |
Model FP-1520
Fluorescence Detector |
6738-J002A |
Model UV-970M
Multichannel UV Detector |
6726-J002A |
Model RI-930 Refractive
Index Detector |
6734-J002A |
Model CL-925
Chemiluminescence Detector |
6763-J002B |
Model CD-1595 Circular
Dichroism Chiral Detector |
6728-J002A |
Model CR-990 Chiral
Polarimetric Detector |
6785-J002A |
Model CO-1560 Column
Oven |
6705-H111A |
Cooling standard vial
rack, 50 vials |
6705-H112B |
Cooling eppendorf tube
rack, 50 vials |
6705-2018GA |
Cooling rack adaptor for
6705-H111A and 6705-H112B |
6705-H113A |
Cooling Chromacol vial
rack for 06-CTV(A), 84 vials |
6705-H114A |
Cooling Chromacol vial
rack for 03-CVG, 84 vials |
6705-H119A |
Cooling rack adaptor for
6705-H113A and 6705-H114A |
6705-H136A |
Cooling microplate rack
including rack and acryl cover |
6561-H103A |
Standard sample vial
set, 1.5 ml. 64 btls/set, with cap and gasket |
6561-H108A |
Standard sample vial set
(amber), 1.5 ml, 64 btls/set, with cap and gasket |
6561-H104A |
Micro sample vial set,
0.3 ml, 50btls/set, with holder, cap and gasket |
0410-0039 |
Screw cap vial, 1.5 ml,
500 btls/set, 2-SV |
0410-0041 |
Screw cap vial, (amber),
1.5 ml, 250 btls/set, 2-SV(A) |
0410-0042 |
Screw cap vial (amber),
1.5 ml, 500 btls/set, 2-SV(A) |
0410-0045 |
Screw cap vial, 1.0 ml,
500 btls/set, 1,1STVG |
0410-0031 |
Crimp-top vial, 1.0 ml,
500 btls/set, 03-CVG |
0410-0055 |
Crimp-top vial (amber),
0.4 ml, 500 btls/set, 06-CTV(A) |
0402-0039 |
Crimp-top vial with
septum, 1000
pcs/set | |